Microwave irradiation synthesis of 4-sulfo-1,8-naphthalimide in Zn(OAc)2 /EtOH-H2 O (2019)
- Authors:
- USP affiliated authors: TRIBONI, EDUARDO REZENDE - EEL ; IZÁRIO FILHO, HÉLCIO JOSÉ - EEL ; BARBOZA, JAYNE CARLOS DE SOUZA - EEL ; POLITI, MARIO JOSE - IQ ; SILVA, OTÁVIO AUGUSTO DA - EEL ; SANTANA, CATHERINE GAZOLLA - EEL
- Unidades: EEL; IQ
- Assunto: ENGENHARIA QUÍMICA
- Keywords: N-substituted 4-sulfo-1,8-naphthalimides; microwave reactor; Lewis catalysis Zn(OAc)2; H2O-EtOH binary solvent
- Agências de fomento:
- Language: Inglês
- Abstract: The synthesis of N-substituted 4-sulfo-1,8-naphthalimide derivatives was performed in microwave reactor. The reaction was conducted in binary solvent mixture (EtOH:H2 O 1:1 v:v) with 4-sulfo-1,8-naphtalic anhydride, the respective primary amine, and Zn(OAc)2 as a catalyst. High yields in a short reaction time were achieved (> 80 % in 5 min). The Lewis acid catalyst and the binary mixture have an important role on the reactivity and time reaction.
- Imprenta:
- Source:
- Título do periódico: Journal of Chemical Technology and Metallurgy
- ISSN: 1314-7978
- Volume/Número/Paginação/Ano: v.54, n.2, p.260-265, 2019
-
ABNT
SANTANA, Catherine Gazolla et al. Microwave irradiation synthesis of 4-sulfo-1,8-naphthalimide in Zn(OAc)2 /EtOH-H2 O. Journal of Chemical Technology and Metallurgy, v. 54, n. 2, p. 260-265, 2019Tradução . . Disponível em: https://journal.uctm.edu/node/j2019-2/2_18-80_p260-265.pdf. Acesso em: 27 abr. 2024. -
APA
Santana, C. G., Silva, O. A. da, Izario Filho, H. J., Barboza, J. C. de S., Politi, M. J., & Triboni, E. R. (2019). Microwave irradiation synthesis of 4-sulfo-1,8-naphthalimide in Zn(OAc)2 /EtOH-H2 O. Journal of Chemical Technology and Metallurgy, 54( 2), 260-265. Recuperado de https://journal.uctm.edu/node/j2019-2/2_18-80_p260-265.pdf -
NLM
Santana CG, Silva OA da, Izario Filho HJ, Barboza JC de S, Politi MJ, Triboni ER. Microwave irradiation synthesis of 4-sulfo-1,8-naphthalimide in Zn(OAc)2 /EtOH-H2 O [Internet]. Journal of Chemical Technology and Metallurgy. 2019 ;54( 2): 260-265.[citado 2024 abr. 27 ] Available from: https://journal.uctm.edu/node/j2019-2/2_18-80_p260-265.pdf -
Vancouver
Santana CG, Silva OA da, Izario Filho HJ, Barboza JC de S, Politi MJ, Triboni ER. Microwave irradiation synthesis of 4-sulfo-1,8-naphthalimide in Zn(OAc)2 /EtOH-H2 O [Internet]. Journal of Chemical Technology and Metallurgy. 2019 ;54( 2): 260-265.[citado 2024 abr. 27 ] Available from: https://journal.uctm.edu/node/j2019-2/2_18-80_p260-265.pdf - Microwave irradiation synthesis of 4-sulfo-1,8-naphthalimide in Zn(OAc)'IND. 2' /EtOH-'H IND. 2'O
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